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Thorough study of one’s TEM photographs (G) out of graphite needles within the trials broadening immediately after 8 minute regarding the next increasing processes from the 1,600 W obviously showcases the brand new phase conversion techniques away from graphite to help you diamond. The fresh white packets would be the portion to your involved increased photographs and you can FFT photographs less than, plus the reddish and white arrows mean the newest flat point. (H) and you will (H-1) is the HADDF and you can brilliant profession TEM photographs for another graphite needle, correspondingly, for the related increased images and you can FFT pictures lower than. The brand new EELS spectra (I) of your own various other sites noted by reddish points from various other phase converting needle revealed within the (H)/(H-1).
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(J)/(J-1) Sketch of the phase transformation away from graphite in order to diamond on the graphite needle person on the cauliflower-for example particles. To learn it incredible periodicity evolving procedure, HRTEM specifications to the recently molded layer was did (Fig. 2). The new 0-s try (Fig. 2A) displays highest rod-such as diamond crystals confirmed by diffraction places in the diamond (111) orientation regarding the inset Fourier changes (FFT) picture.
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